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Pesticide Analysis

PrimusLabs.com utilizes current FDA, PAM, EPA and AOAC methodologies for its pesticide analyses. These, coupled with our internal Standard Operating Procedures (SOP), adherence to the Chain of Custody for all samples from sample collection to analysis, the use of high quality, high purity analytical standards, utilization of quality equipment such as gas chromatographs (GC) and high performance liquid chromatographs (HPLC), ensure accurate and reproducible analyses.

The equipment used by PrimusLabs.com is configured for the detection of organochlorines, organophosphates, organonitrates, organosulfates and methyl carbamates. Based upon the extraction methods and equipment utilized, well over 250 compounds as listed in the FDA's Pesticide Analytical Manual Vol. I Table 302-A can be analyzed for and recovered by PrimusLabs.com. Utilizing all of the above and employing highly qualified, well-trained and dedicated personnel assures that the client obtains accurate and timely analytical results.
Click here to see List of Compounds in a Multi-Residue Screen

The PrimusLabs.com pesticide residue analysis program consists of three subgroups:
Certified A "Certified" program is a pre-harvest sampling and analysis program in which PrimusLabs.com personnel collect a representative sample of the commodity from the field and maintain a strict chain of custody from the field to the laboratory for analysis. A product is "Certified" when it meets applicable government standards.
Click here to see List of Certified Whole Commodities
Inspected The "Inspected" program is a post-harvest sampling and analysis program in which PrimusLabs.com personnel collect a representative sample from the loading dock, cooler or distribution center, again utilizing the chain of custody from the sample collection point to the laboratory. Based upon favorable findings, this program can warrant that any pesticide residues detected within the lot analyzed are within established government tolerances.
Tested A "Tested" program is available to any individual or firm concerned with possible pesticide residues that may be present on a specific shipment or commodity. A sample is provided to PrimusLabs.com by the client, analyzed and the results are then reported to the client.
Guidelines for Sampling to be Performed by the Client • Field Sampling for Pesticide Analysis (PDF)
• Soil Sampling for Pesticide Analysis (PDF)
• Sample Packing and Shipping Instructions (PDF)

     * Click here to request Laboratory Analysis Services
Micro Analysis

The PrimusLabs.com microbial analysis:
Environment PrimusLabs.com offers a wide range of microbiological services including Total Plate Count, Listeria and Yeast & Mold analyses for determination of environmental cleanliness.
Water sources PrimusLabs.com offers certified water testing for Total Coliform and E.coli to determine water quality.
Final product PrimusLabs.com offers a comprehensive range of microbiological services including Total Plate Count, Total Coliform, E.coli and Yeast & Mold analyses for determination of product quality. Additionally, analyses for specific pathogens such as Salmonella, E.coli 0157:H7, Listeria, Staphylococcus aureus, Clostridium perfringens, Shigella and many others can be performed ensuring product safety.
Special Services PrimusLabs.com also performs shelf life and challenge studies, sensory evaluations of food products and can assist in determining the cause of spoilage problems.
Guidelines for Sampling to be Performed by the Client • Compost–Soil Amendments Sampling (PDF)
• Field Sampling CA–LGMA Protocol (PDF)
• Field Sampling for Microbiological Analysis (PDF)
• Listeria Sampling – Swab Method (PDF)

• Listeria Sampling – Sponge Method (PDF)
• Microbiological SWABS Using RediSwabs (PDF)
• Water Sampling for Microbiological Analysis (PDF)
• Sample Packing & Shipping Instructions (PDF)

     * Click here to request Laboratory Analysis Services

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   Multi-Residue Screen
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A) Halogenated Pesticides
Acetamiprid Chlorobenzilate Dimethomorph Iprodione Procymidone
Alachlor Chlorothalonil Endosulfan I Lambda-Cyhalothrin Pronamide
Aldrin Chloroxuron Endosulfan II Lindane Propachlor
Anilazine Chlorpropham Endosulfan Sulfate Linuron Propanil
Atrazine Cyanazine Endrin Metolachlor Propiconazole
Benzoylprop-ethyl Cyfluthrin Esfenvalerate Methoxychlor Pyraclostrobin
BHC, alpha Cypermethrin Etaconazole Mirex Pyridaben
BHC, beta Cyproconazole Ethylan Monolinuron Pyrifenox
BHC, delta DCPA (Dacthal) Fenarimol Myclobutanil Quinoxyfen
Bifenox DDD Fenazaquin Nitrofen Simazine
Bifenthrin DDE Fenbuconazole Nuarimol Simetryn
Boscalid DDT Fenhexamid Ofurace Tebuconazole
Bromacil Deltamethrin Fenson Oxadiazon Terbacil
Butachlor Dichlobenil Fenvalerate Oxadixyl Tetradifon
Captafol Dichlofluanid Fuchloralin Oxyfluorfen Thiobencarb
Captan Dichlone Folpet PCNB (Quintozene) Tolylfluanid
Carfentrazone-ethyl Diclobutrazol Flucythrinate Paclobutrazol Toxaphene
Chlordane Dicloran Heptachlor Penconazole Tralomethrin
Chlordimeform Dicofol Heptachlor epoxide Pentachloroaniline Triadimefon
Chlorfenapyr Dieldrin Hexachlorobenzene Permethrin Triadimenol
Chlorfenson Diethatyl-ethyl Hexaconazole Perthane Triflumizole
Chlornitrofen Difenconazole Imazalil Phosalone Vegadex
Chloroneb Dimethachlor Indoxacarb Prochloraz Vinclozolin
B) Organophosphate Pesticides
Acephate Demeton-o Fenitrothion Mevinphos Prothiofos
Azinphos-ethyl Demeton-s Fensulfothion Moncrotophos Prothoate
Azinphos-methyl Demeton-s-sulfone Fenthion Naled Pyrazophos
Bensulide Dialifos Fonofos Omethoate Pyridaphenthion
Bromophos Diazinon Formothion Parathion Quinalphos
Bromophos-ethyl Dichlorvos Heptenophos Parathion-methyl Ronnel
Cadusafos Dicrotophos Iprobenfos Phenthoate Sulprofos
Carbophenothion Dimethoate Isazophos Phorate Terbufos
Carbophenothion OA Dioxathion Isofenphos Phosalone Tetrachlorvinphos
Chlorfenvinphos Disulfoton Leptophos Phosfolan Thiometon
Chlorpyrifos Disulfoton-sulfone Malathion Phosmet Thionazin
Chlorpyrifos-methyl Edifenphos Malaoxon Phosphamidon Toclofos-methyl
Chlorthiophos EPN Metasystox-R Piperophos Triazophos
Coumaphos Ethion Methacrifos Pirimiphos
Crotoxyphos Ethoprop Methamidophos Pirimiphos-methyl
Cyanophos Etrimfos Methidathion Profenofos
DEF Fenamiphos Methyl Trithion Propetamphos
C) Methyl Carbamates
Aldicarb Bendiocarb 3-keto Carbofuran Methiocarb sulfone Propoxur
Aldicarb sulfone Bufencarb Ethiofencarb Methiocarb sulfoxide Thiodicarb
Alidicarb sulfoxide Carbaryl Fenobucarb Methomyl  
Aminocarb Carbofuran Methiocarb Oxamyl  
SPECIAL ANALYSES (Upon request)
D) Pesticides Containing Nitrogen/Sulfur
Acrinathrin Chlorfenapyr Fenpropathrin Mexacarbate Pymetrozine
Ametryn Chlozolinate Fenpropimorph Napropamide Pyrethrins
Azoxystrobin Cycloate Fipronil Norflurazon Pyrifenox
Benalaxyl Cyprodinil Fludioxonil Oryzalin Pyrimethanil
Benefin Dimethametryn Flurochloridone Pendimethalin Pyriproxyfen
Benfluralin Diphenamid Fluzilazole o-Phenylphenol Quinomethionate
Biphenyl Diphenylamine Furalaxyl Pirimicarb Tebufenpyrad
Bitertanol EPTC Kresoxim-methyl Profluralin Tecnazene
Bromopropylate Ethalfluralin Mecarbam Promecarb Tefluthrin
Bupirimate Ethirimol Metalaxyl Prometon Thiabendazole
Buprofezin Ethofumesate Metazachlor Prometryn Tolylfluanid
Carbetamide Ethoxyquin Methoprotryn Propargite Trifloxystrobin
Carbosulfan Fenamidone Metribuzin Propham Trifluralin
E) Dithiocarbamates analysis (EBDCs and related compounds*)
Ferbam Mancozeb Maneb Metham-sodium Thiram
Zineb Ziram
*results reported as CS2
F) Benzimidazoles
Benomyl Carbendazim Thiabendazole Thiophanate-methyl  
G) Chlorophenoxies and related compounds
2,4,5-T 2,4,5-TP 2,4-D 2,4-DB Bromoxynil
Dicamba Dichlorprop Diclofop-methyl Fluazifop-butyl MCPA
MCPB Silvex
H) Sulfur and its oxidative derivatives
Sulfate Sulfite Sulfur    
I) Alar (Daminozide)
         
J) Diuron (Karmex)
         
K) Triclopyr
         
L) Patulin
         
M) Fenbutatin-oxide (Vendex)
         
N) Oxydemeton-methyl, MetaSystox-R (MSR)
         
O) Spinosad
         
P) Glyphosate, AMPA)
         
Q) Imidacloprid
         
R) Thidiazuron
         
S) Clopyralid
         
T) Dinotefuran
         
U) Thiamethoxam
         
V) Methoxyfenozide
         
NOTE:
 If a compound of interest does not appear on the list, please inquire. It may be possible to incorporate the compound into a screen. In situations where the compound cannot be tested through a multiresidue screen, PrimusLabs.com welcomes inquiries regarding individual specialized analysis.

 FDA's multiresidue methods (MRMs) as described in the Pesticide Analytical Manual (PAM) Volume I are used for multiresidue analyses. Gas and Liquid chromatographic systems are used in the analyses. Confirmation of violative residues using mass spectrometer detection is done as complimentary test.

 Pesticide Residue Testing Accreditations:State of California, Department of Health Services - Environmental Laboratory Certification #1954.Japanese Ministry of Health, Labour and Welfare Registered Foreign Laboratory.

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